Synthesis of [2,3,4,5,6-2H5]phenyl glucosinolate

Jason B. Bialecki, Josef Ruzicka, Athula B. Attygalle

Research output: Contribution to journalArticlepeer-review

6 Scopus citations

Abstract

Starting from commercially available [2,3,4,5,6-2H 5]benzoic acid, [2,3,4,5,6-2H5]phenyl glucosinolate was synthesized. Under negative-ion electrospray-ionization mass spectrometric conditions, this compound affords a peak at m/z 399. Since this m/z value is not known from the ions derived from natural glucosinolates, the [2,3,4,5,6-2H5]phenyl glucosinolate reported here is useful as an internal standard for the quantification of glucosinolates by negative-ion mass spectrometry (MS) and liquid chromatography (LC)/MS techniques.

Original languageEnglish
Pages (from-to)711-715
Number of pages5
JournalJournal of Labelled Compounds and Radiopharmaceuticals
Volume50
Issue number8
DOIs
StatePublished - Jul 2007

Keywords

  • Collision-induced dissociation (CID)
  • Electrospray-ionization mass spectrometry
  • Glucosinolates
  • Internal standard
  • Phenyl glucosinolate

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